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    Nickel-Catalyzed Synthesis of Silanes from Silyl Ketones

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    Manuscript_revised.pdf
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    Description:
    Accepted manuscript
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    Type
    Article
    Authors
    Srimontree, Watchara
    Lakornwong, Waranya
    Rueping, Magnus cc
    KAUST Department
    Chemical Science Program
    KAUST Catalysis Center (KCC)
    Physical Science and Engineering (PSE) Division
    Date
    2019-11-08
    Embargo End Date
    2020-11-08
    Permanent link to this record
    http://hdl.handle.net/10754/660228
    
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    Abstract
    An unprecedented nickel-catalyzed decarbonylative silylation via CO extrusion intramolecular recombination fragment coupling of unstrained and nondirecting group-Assisted silyl ketones is described. The inexpensive and readily available catalyst performs under mild reaction conditions and enables the synthesis of structurally diverse arylsilanes, including heterocyclic and natural product derivatives.
    Citation
    Srimontree, W., Lakornwong, W., & Rueping, M. (2019). Nickel-Catalyzed Synthesis of Silanes from Silyl Ketones. Organic Letters. doi:10.1021/acs.orglett.9b03487
    Sponsors
    W.L. was supported by the Thailand Research Fund through the Royal Golden Jubilee Ph.D. Program for the one-year exchange fellowship to RWTH-Aachen University. We thank Tengfei Ji for performing the large scale experiment.
    Publisher
    American Chemical Society (ACS)
    Journal
    Organic Letters
    DOI
    10.1021/acs.orglett.9b03487
    Additional Links
    https://pubs.acs.org/doi/10.1021/acs.orglett.9b03487
    ae974a485f413a2113503eed53cd6c53
    10.1021/acs.orglett.9b03487
    Scopus Count
    Collections
    Articles; Physical Science and Engineering (PSE) Division; Chemical Science Program; KAUST Catalysis Center (KCC)

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