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    ZIF-78 membrane derived from amorphous precursors with permselectivity for cyclohexanone/cyclohexanol mixture

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    Type
    Article
    Authors
    Fan, Lili
    Xue, Ming
    Kang, Zixi
    Wei, Guoying
    Huang, Lin
    Shang, Jiushu
    Zhang, Daliang cc
    Qiu, Shilun
    KAUST Grant Number
    CRG-1-2012-LAI-009
    Date
    2014-07
    Permanent link to this record
    http://hdl.handle.net/10754/600204
    
    Metadata
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    Abstract
    Cyclohexanone and cyclohexanol are products of selective oxidation of cyclohexane. They are important industrial intermediates and difficult to be separated due to their close boiling points. In this work, well-intergrown ZIF-78 membrane was successfully synthesized on the porous silica substrate by secondary growth method and applied for separation of cyclohexanone/cyclohexanol mixture for the first time. Meanwhile, a facile method for seeding procedure was developed by utilizing the amorphous ZIF-78 precursors to provide better-distributed nucleation sites. Both XRD and SEM results confirmed the good quality of the membrane. The pervaporation separation of cyclohexanone/ cyclohexanol mixture were carried out at room temperature with permselectivity of 1:2 and total flux around 8.7 × 10-2 kg m-2 h-1. © 2013 Elsevier Inc. All rights reserved.
    Citation
    Fan L, Xue M, Kang Z, Wei G, Huang L, et al. (2014) ZIF-78 membrane derived from amorphous precursors with permselectivity for cyclohexanone/cyclohexanol mixture. Microporous and Mesoporous Materials 192: 29–34. Available: http://dx.doi.org/10.1016/j.micromeso.2013.11.008.
    Sponsors
    This work was supported by the National Basic Research Program of China (2011CB808703, 2012CB821700), the National Natural Science Foundation of China (Grant nos. 91022030, 21101072, 21261130584), "111" project (B07016), Award Project of KAUST (CRG-1-2012-LAI-009) and Zhuhai Science and Technology Department Project (2011A050101008, 2012D0501990028).
    Publisher
    Elsevier BV
    Journal
    Microporous and Mesoporous Materials
    DOI
    10.1016/j.micromeso.2013.11.008
    ae974a485f413a2113503eed53cd6c53
    10.1016/j.micromeso.2013.11.008
    Scopus Count
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