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    Efficient and Highly Aldehyde Selective Wacker Oxidation

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    Type
    Article
    Authors
    Teo, Peili
    Wickens, Zachary K.
    Dong, Guangbin
    Grubbs, Robert H.
    Date
    2012-06-13
    Online Publication Date
    2012-06-13
    Print Publication Date
    2012-07-06
    Permanent link to this record
    http://hdl.handle.net/10754/598098
    
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    Abstract
    A method for efficient and aldehyde-selective Wacker oxidation of aryl-substituted olefins using PdCl 2(MeCN) 2, 1,4-benzoquinone, and t-BuOH in air is described. Up to a 96% yield of aldehyde can be obtained, and up to 99% selectivity can be achieved with styrene-related substrates. © 2012 American Chemical Society.
    Citation
    Teo P, Wickens ZK, Dong G, Grubbs RH (2012) Efficient and Highly Aldehyde Selective Wacker Oxidation. Organic Letters 14: 3237–3239. Available: http://dx.doi.org/10.1021/ol301240g.
    Sponsors
    We gratefully acknowledge financial support from King Abdullah University of Science and Technology Centre in Development, King Fahd University of Petroleum and Minerals, and the NSF. G.D. thanks the Camille and Henry Dreyfus Foundation for a postdoctoral fellowship.
    Publisher
    American Chemical Society (ACS)
    Journal
    Organic Letters
    DOI
    10.1021/ol301240g
    PubMed ID
    22694293
    ae974a485f413a2113503eed53cd6c53
    10.1021/ol301240g
    Scopus Count
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