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We are grateful for helpful discussions with Dr. Jian He, and also the synthesis techniques developed by Jennifer Graff. We would like to acknowledge the support of a Faculty Initiated Collaboration (FIC) grant from the King Abdullah University of Science and Technology (KAUST) and previous support for much of the equipment from a DOE grant that is supported by a DOE/EPSCoR Implementation Grant (#DE-FG02-04ER46139), and the SC EPSCoR cost-sharing program.