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    A Toolbox of Solid-State NMR Experiments for the Characterization of Soft Organic Nanomaterials

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    Manuscript_SoftMaterials_Straasoe-Saleem-Hansen.pdf
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    4.186Mb
    Format:
    PDF
    Description:
    Accepted Manuscript
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    Type
    Article
    Authors
    Straasø, Lasse Arnt
    Saleem, Qasim
    Hansen, Michael Ryan
    KAUST Department
    KAUST Solar Center (KSC)
    Physical Science and Engineering (PSE) Division
    Date
    2016-02-02
    Online Publication Date
    2016-02-02
    Print Publication Date
    2016
    Permanent link to this record
    http://hdl.handle.net/10754/597175
    
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    Abstract
    Determining how organic molecules self-assemble into a solid material is a challenging and demanding task if a single crystal of the material cannot be produced. Solid-state NMR spectroscopy offers access to such molecular details via an appropriate selection of techniques. This report gives a selected overview of 1D and 2D solid-state NMR techniques for elucidating the structure of soft organic solids. We focus on how the solid-state NMR techniques are designed from the perspective of the different nuclear interactions, using average Hamiltonian theory and product operators. We also introduce recent methods for quantification and reduction of experimental artifacts. Finally, we highlight how the solid-state NMR techniques can be applied to soft organic materials by reviewing recent applications to semicrystalline polymers, π-conjugated polymers, natural silk, and graphene-related materials.
    Citation
    Straasø, L.A., Saleem, Q. and Hansen, M.R., 2016. A Toolbox of Solid-State NMR Experiments for the Characterization of Soft Organic Nanomaterials. Annual Reports on NMR Spectroscopy.
    Publisher
    Elsevier BV
    Journal
    Annual Reports on NMR Spectroscopy
    DOI
    10.1016/bs.arnmr.2015.12.001
    Additional Links
    http://www.sciencedirect.com/science/article/pii/S006641031500068X
    ae974a485f413a2113503eed53cd6c53
    10.1016/bs.arnmr.2015.12.001
    Scopus Count
    Collections
    Articles; Physical Science and Engineering (PSE) Division; KAUST Solar Center (KSC)

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