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    Rapid continuous flow synthesis of high-quality silver nanocubes and nanospheres

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    Type
    Article
    Authors
    Mehenni, Hakim
    Sinatra, Lutfan cc
    Mahfouz, Remi cc
    Katsiev, Khabiboulakh
    Bakr, Osman cc
    KAUST Department
    Functional Nanomaterials Lab (FuNL)
    KAUST Catalysis Center (KCC)
    KAUST Solar Center (KSC)
    Material Science and Engineering Program
    Physical Science and Engineering (PSE) Division
    Date
    2013
    Permanent link to this record
    http://hdl.handle.net/10754/562541
    
    Metadata
    Show full item record
    Abstract
    We report a biphasic-liquid segmented continuous flow method for the synthesis of high-quality plasmonic single crystal silver nanocubes and nanospheres. The nanocubes were synthesized with controllable edge lengths from 20 to 48 nm. Single crystal nanospheres with a mean size of 29 nm were obtained by in-line continuous-flow etching of as-produced 39 nm nanocubes with an aqueous solution of FeNO3. In comparison to batch synthesis, the demonstrated processes represent highly scalable reactions, in terms of both production rate and endurance. The reactions were conducted in a commercially available flow-reactor system that is easily adaptable to industrial-scale production, facilitating widespread utilization of the procedure and the resulting nanoparticles. This journal is © The Royal Society of Chemistry 2013.
    Citation
    Mehenni, H., Sinatra, L., Mahfouz, R., Katsiev, K., & Bakr, O. M. (2013). Rapid continuous flow synthesis of high-quality silver nanocubes and nanospheres. RSC Advances, 3(44), 22397. doi:10.1039/c3ra43295e
    Sponsors
    The authors acknowledge the use of KAUST's Core Labs and the support of KAUST's University Research Fund.
    Publisher
    Royal Society of Chemistry (RSC)
    Journal
    RSC Advances
    DOI
    10.1039/c3ra43295e
    ae974a485f413a2113503eed53cd6c53
    10.1039/c3ra43295e
    Scopus Count
    Collections
    Articles; Physical Science and Engineering (PSE) Division; Material Science and Engineering Program; KAUST Catalysis Center (KCC); KAUST Solar Center (KSC)

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