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    Shape- and morphology-controlled sustainable synthesis of Cu, Co, and in metal organic frameworks with high CO2 capture capacity

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    Type
    Article
    Authors
    Sarawade, Pradip
    Tan, Hua
    Polshettiwar, Vivek cc
    KAUST Department
    Analytical Chemistry Core Lab
    Computational Bioscience Research Center (CBRC)
    KAUST Catalysis Center (KCC)
    Physical Science and Engineering (PSE) Division
    Date
    2012-11-06
    Online Publication Date
    2012-11-06
    Print Publication Date
    2013-01-07
    Permanent link to this record
    http://hdl.handle.net/10754/562402
    
    Metadata
    Show full item record
    Abstract
    We studied the effects of various surfactants on the shape and morphology of three metal organic frameworks (MOFs), i.e., Co-MOF, Cu-MOF, and In-MOF, which were synthesized under microwave irradiation. The as-synthesized materials were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and nitrogen sorption. The effects of microwave irradiation time, temperature, and surfactant template were investigated. The synthetic parameters, including the type of surfactant template and the reaction temperature, played crucial roles in the size, shape, and morphology of the MOF microcrystals. We also evaluated these MOFs as sorbents for capturing CO2. Of the synthesized materials, Cu-MOF demonstrated the highest CO2 capture capacity, even at atmospheric pressure and ambient temperature. © 2012 American Chemical Society.
    Citation
    Sarawade, P., Tan, H., & Polshettiwar, V. (2012). Shape- and Morphology-Controlled Sustainable Synthesis of Cu, Co, and In Metal Organic Frameworks with High CO2 Capture Capacity. ACS Sustainable Chemistry & Engineering, 1(1), 66–74. doi:10.1021/sc300036p
    Sponsors
    We thank King Abdullah University of Science and Technology (KAUST) for their funding and support. We also thank Prof. Mohamed Eddaoudi for his lecture on MOFs, which inspired us to engage in this work.
    Publisher
    American Chemical Society (ACS)
    Journal
    ACS Sustainable Chemistry & Engineering
    DOI
    10.1021/sc300036p
    ae974a485f413a2113503eed53cd6c53
    10.1021/sc300036p
    Scopus Count
    Collections
    Articles; Analytical Chemistry Core Lab; Physical Science and Engineering (PSE) Division; KAUST Catalysis Center (KCC); Computational Bioscience Research Center (CBRC)

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