Using a precursor in lamellar structure for the synthesis of uniform ZnS nanocrystals

Handle URI:
http://hdl.handle.net/10754/561919
Title:
Using a precursor in lamellar structure for the synthesis of uniform ZnS nanocrystals
Authors:
Xu, Xinjiang; Jiang, Shunping; Wu, Xiaoyuan; Chang, Jinjing; Xu, Jiangping
Abstract:
Uniform ZnS nanocrystals of about 15 nm were prepared through a low temperature hydrothermal approach by treating Zn-PhPO nanosheets with Na 2S aqueous solution. Both the precursor and the final product were studied by the means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The photo-luminescent spectrum of the synthesized ZnS nanocrystals showed their good crystalline nature. Based on this study, the precursor structure-controlling effect was discussed, and in addition, the relevant factors possibly affecting the particle formation and the growth possessed were applied in the discussion to interpret the transformation mechanism. Further research showed that both the structure characters of the precursors and the mass transportation which occurred during the synthesis greatly affected the morphology and organization state of the final products. This research may provide some facts on the structure-controlling approaches along with a general method for the preparation of uniform sulfide nanocrystals. © Springer Science+Business Media B.V. 2011.
KAUST Department:
Computer, Electrical and Mathematical Sciences and Engineering (CEMSE) Division; Physical Sciences and Engineering (PSE) Division
Publisher:
Springer Verlag
Journal:
Research on Chemical Intermediates
Issue Date:
12-Nov-2011
DOI:
10.1007/s11164-011-0437-1
Type:
Article
ISSN:
09226168
Sponsors:
This research was supported by the Startup research fund and Key project from Yulin Normal University (X.-J. Xu).
Appears in Collections:
Articles; Physical Sciences and Engineering (PSE) Division; Computer, Electrical and Mathematical Sciences and Engineering (CEMSE) Division

Full metadata record

DC FieldValue Language
dc.contributor.authorXu, Xinjiangen
dc.contributor.authorJiang, Shunpingen
dc.contributor.authorWu, Xiaoyuanen
dc.contributor.authorChang, Jinjingen
dc.contributor.authorXu, Jiangpingen
dc.date.accessioned2015-08-03T09:34:07Zen
dc.date.available2015-08-03T09:34:07Zen
dc.date.issued2011-11-12en
dc.identifier.issn09226168en
dc.identifier.doi10.1007/s11164-011-0437-1en
dc.identifier.urihttp://hdl.handle.net/10754/561919en
dc.description.abstractUniform ZnS nanocrystals of about 15 nm were prepared through a low temperature hydrothermal approach by treating Zn-PhPO nanosheets with Na 2S aqueous solution. Both the precursor and the final product were studied by the means of X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The photo-luminescent spectrum of the synthesized ZnS nanocrystals showed their good crystalline nature. Based on this study, the precursor structure-controlling effect was discussed, and in addition, the relevant factors possibly affecting the particle formation and the growth possessed were applied in the discussion to interpret the transformation mechanism. Further research showed that both the structure characters of the precursors and the mass transportation which occurred during the synthesis greatly affected the morphology and organization state of the final products. This research may provide some facts on the structure-controlling approaches along with a general method for the preparation of uniform sulfide nanocrystals. © Springer Science+Business Media B.V. 2011.en
dc.description.sponsorshipThis research was supported by the Startup research fund and Key project from Yulin Normal University (X.-J. Xu).en
dc.publisherSpringer Verlagen
dc.subjectCrystal growthen
dc.subjectHydrothermalen
dc.subjectNanomaterialsen
dc.subjectStructure-controlleden
dc.titleUsing a precursor in lamellar structure for the synthesis of uniform ZnS nanocrystalsen
dc.typeArticleen
dc.contributor.departmentComputer, Electrical and Mathematical Sciences and Engineering (CEMSE) Divisionen
dc.contributor.departmentPhysical Sciences and Engineering (PSE) Divisionen
dc.identifier.journalResearch on Chemical Intermediatesen
dc.contributor.institutionCollege of Chemistry and Material, Yulin Normal University, 299# Middle Jiaoyu Road, Yulin 537000, Guangxi, Chinaen
dc.contributor.institutionKey Laboratory of Fujian Province, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Science, Fuzhou 350002, Fujian, Chinaen
kaust.authorXu, Jiangpingen
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